7UC6
Stat5a Core in complex with Compound 12
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-F |
Synchrotron site | APS |
Beamline | 21-ID-F |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2021-03-24 |
Detector | RAYONIX MX-300 |
Wavelength(s) | 0.9787 |
Spacegroup name | H 3 2 |
Unit cell lengths | 237.674, 237.674, 112.811 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.820 - 3.101 |
R-factor | 0.1972 |
Rwork | 0.195 |
R-free | 0.24290 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.020 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.4 (3-FEB-2022)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 3.150 |
High resolution limit [Å] | 3.100 | 8.400 | 3.100 |
Rmerge | 0.130 | 0.031 | 1.403 |
Rmeas | 0.136 | 0.032 | 1.468 |
Rpim | 0.040 | 0.010 | 0.433 |
Total number of observations | 253749 | ||
Number of reflections | 22212 | 1168 | 1110 |
<I/σ(I)> | 5.3 | ||
Completeness [%] | 100.0 | 99.9 | 100 |
Redundancy | 11.4 | 10.5 | 11.5 |
CC(1/2) | 0.999 | 0.912 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 1.1M Sodium Malonate pH 7.0, 0.1M Hepes pH 7.0, 0.5% Jeffamine ED-2001 pH 7.0 |