7U3O
[a2T7] Self-assembling asymmetric tensegrity triangle with P1 symmetry
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-09-25 |
Detector | DECTRIS EIGER2 X 9M |
Wavelength(s) | 1.00743 |
Spacegroup name | P 1 |
Unit cell lengths | 67.409, 68.154, 68.771 |
Unit cell angles | 101.47, 99.06, 97.84 |
Refinement procedure
Resolution | 40.960 - 3.310 |
R-factor | 0.2306 |
Rwork | 0.229 |
R-free | 0.25610 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3gbi |
RMSD bond length | 0.009 |
RMSD bond angle | 1.049 |
Data reduction software | autoPROC |
Data scaling software | STARANISO |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 65.781 | 65.781 | 3.920 |
High resolution limit [Å] | 3.310 | 11.119 | 3.310 |
Number of reflections | 8803 | 440 | 441 |
<I/σ(I)> | 6 | ||
Completeness [%] | 84.7 | ||
Redundancy | 3.6 | 3.7 | 3.8 |
CC(1/2) | 0.998 | 0.997 | 0.615 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 277 | 100 mM MOPS, 1.25 M magnesium sulfate, sodium hydroxide |