7U1Z
Crystal structure of the DRBD and CROPs of TcdA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-08-07 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9791 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 379.507, 187.641, 95.324 |
Unit cell angles | 90.00, 101.30, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 186.100 | 3.290 |
High resolution limit [Å] | 3.180 | 3.180 |
Rmerge | 0.283 | 1.140 |
Number of reflections | 108739 | 10768 |
<I/σ(I)> | 4.43 | |
Completeness [%] | 99.1 | |
Redundancy | 3.5 | |
CC(1/2) | 0.944 | 0.380 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | 0.1 M Bis-Tris pH 6.3, 0.6 M lithium sulfate |