7T2M
Crystal Structure of TEAD2 in a covalent complex with TED-664
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | CMOS |
Collection date | 2021-04-15 |
Detector | RDI CMOS_8M |
Wavelength(s) | 1.07216 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 111.106, 61.570, 79.511 |
Unit cell angles | 90.00, 112.69, 90.00 |
Refinement procedure
Resolution | 52.780 - 2.810 |
R-factor | 0.2242 |
Rwork | 0.221 |
R-free | 0.27890 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6e5g |
RMSD bond length | 0.010 |
RMSD bond angle | 1.067 |
Data reduction software | XDS |
Data scaling software | STARANISO |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 52.780 | 3.110 |
High resolution limit [Å] | 2.810 | 2.810 |
Rmeas | 0.163 | 1.077 |
Rpim | 0.084 | 0.560 |
Number of reflections | 7956 | 398 |
<I/σ(I)> | 5.7 | 1.2 |
Completeness [%] | 89.9 | 59.8 |
Redundancy | 3.7 | 3.7 |
CC(1/2) | 0.993 | 0.501 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | Sodium Formate 1.8M - 2.4M HEPES pH 7.2 - 7.4 |