7SZA
Crystal Structure Analysis of human PRPK complex with a compound
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-08-20 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9792 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 297.510, 47.490, 62.270 |
Unit cell angles | 90.00, 96.53, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 73.951 | 73.950 | 1.930 |
High resolution limit [Å] | 1.900 | 5.160 | 1.900 |
Rmeas | 0.071 | 0.023 | 0.933 |
Rpim | 0.037 | 0.012 | 0.484 |
Total number of observations | 12645 | 12318 | |
Number of reflections | 68512 | 3571 | 3358 |
<I/σ(I)> | 13.8 | 39.9 | 1.6 |
Completeness [%] | 99.7 | 99.4 | 99.9 |
Redundancy | 3.7 | 3.5 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.2 | 300 | 100mM Sodium citrate pH 5.2, 12.8% PEG8000, 10mM MgCl2, 10mM TCEP |