7SVO
DPP8 IN COMPLEX WITH LIGAND ICeD-1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-02-03 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9998 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 162.816, 246.016, 261.767 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 135.770 - 2.580 |
R-factor | 0.1804 |
Rwork | 0.180 |
R-free | 0.20760 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6eoo |
RMSD bond length | 0.014 |
RMSD bond angle | 1.742 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 135.780 | 2.830 |
High resolution limit [Å] | 2.580 | 2.580 |
Rmerge | 0.065 | 0.596 |
Number of reflections | 159983 | 38954 |
<I/σ(I)> | 2.23 | |
Completeness [%] | 97.5 | 98.7 |
Redundancy | 3.9 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 0.46 M Nacitrate pH 6.75 |