7SVM
DPP8 IN COMPLEX WITH LIGAND ICeD-2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2019-02-03 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9998 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 162.288, 244.937, 261.487 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 135.290 - 2.690 |
| R-factor | 0.1768 |
| Rwork | 0.176 |
| R-free | 0.21640 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6eoo |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.689 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 135.290 | 2.940 |
| High resolution limit [Å] | 2.690 | 2.690 |
| Rmerge | 0.064 | 0.580 |
| Number of reflections | 138235 | 32528 |
| <I/σ(I)> | 1.97 | |
| Completeness [%] | 96.1 | 97.3 |
| Redundancy | 3 | 2.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 277 | 0.46 M NaCitrate pH 6.75 |
