7SPP
Crystal structure of the SARS-CoV-2 receptor binding domain in complex with VNAR 2C02
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-07-17 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 0.979 |
Spacegroup name | P 21 2 21 |
Unit cell lengths | 61.448, 74.229, 75.456 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.330 | 2.010 |
High resolution limit [Å] | 1.960 | 1.960 |
Rmerge | 0.056 | 1.278 |
Rmeas | 0.065 | |
Rpim | 0.041 | |
Number of reflections | 24971 | 1764 |
<I/σ(I)> | 11.4 | |
Completeness [%] | 98.7 | 98.9 |
Redundancy | 4 | 4 |
CC(1/2) | 0.998 | 0.832 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2 M sodium sulfate and 20 % (w/v) PEG 3350 |