7SN6
U2AF65 UHM BOUND TO SF3B155 ULM5
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-06-25 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.033 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 76.163, 63.156, 49.387 |
Unit cell angles | 90.00, 94.37, 90.00 |
Refinement procedure
Resolution | 37.970 - 1.800 |
R-factor | 0.1834 |
Rwork | 0.180 |
R-free | 0.21690 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4fxw |
Data reduction software | XDS (November 3, 2014) |
Data scaling software | Aimless (0.5.8) |
Phasing software | PHASER |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.970 | 1.840 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.038 | 0.499 |
Rpim | 0.023 | 0.304 |
Number of reflections | 21337 | 1256 |
<I/σ(I)> | 16.7 | 3 |
Completeness [%] | 98.4 | |
Redundancy | 3.6 | 3.6 |
CC(1/2) | 0.990 | 0.920 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 0.1 M SODIUM CITRATE TRIBASIC DIHYDRATE PH 5.6, 15% V/V 2-PROPANOL, 20% PEG 4000 |