7RWW
Crystal structure of a Zn-bound RIDC1 variant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-04-07 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 47.791, 86.913, 49.176 |
Unit cell angles | 90.00, 109.16, 90.00 |
Refinement procedure
Resolution | 35.960 - 1.700 |
R-factor | 0.1765 |
Rwork | 0.175 |
R-free | 0.20770 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2bc5 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.124 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 80.850 | 1.761 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.121 | 0.809 |
Rmeas | 0.126 | 0.849 |
Rpim | 0.032 | 0.341 |
Number of reflections | 40172 | 3987 |
<I/σ(I)> | 11.7 | 3.2 |
Completeness [%] | 99.9 | |
Redundancy | 14.8 | |
CC(1/2) | 0.996 | 0.617 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 295 | 45% MPD, 0.1 M HEPES, 0.2 M MgCl2 |