7R6T
Human EXOG complexed with dRP-containing DNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2021-06-01 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 2 21 |
Unit cell lengths | 73.252, 100.056, 174.902 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.970 - 2.900 |
Rwork | 0.229 |
R-free | 0.28600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5t5c |
RMSD bond length | 0.003 |
RMSD bond angle | 0.535 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.17) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.500 |
High resolution limit [Å] | 2.900 | 2.900 |
Number of reflections | 26817 | 2612 |
<I/σ(I)> | 2.7 | |
Completeness [%] | 99.0 | |
Redundancy | 6.4 | 6.3 |
CC(1/2) | 0.750 | 0.500 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 28% PEG 4K, 0.2 M Ammonium Acetate, 0.1 M Na Citrate tribasic dihydrate pH 5.6 |