7QQE
Nuclear factor one X - NFIX in P41212
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-04-13 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.28199 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 65.009, 65.009, 127.890 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.590 - 3.500 |
R-factor | 0.2247 |
Rwork | 0.223 |
R-free | 0.25890 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7qqd |
RMSD bond length | 0.007 |
RMSD bond angle | 1.031 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.9) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.970 | 3.850 |
High resolution limit [Å] | 3.500 | 3.500 |
Rpim | 0.116 | 0.919 |
Number of reflections | 3802 | 366 |
<I/σ(I)> | 7.6 | 1.3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 25.1 | 26.6 |
CC(1/2) | 0.998 | 0.603 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 0.2 M NaSCN, 20% PEG 3350 |