7QQD
Nuclear factor one X - NFIX in P21
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ELETTRA BEAMLINE 11.2C |
Synchrotron site | ELETTRA |
Beamline | 11.2C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-03-11 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.2705 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 43.171, 98.358, 61.629 |
Unit cell angles | 90.00, 92.70, 90.00 |
Refinement procedure
Resolution | 49.180 - 2.700 |
R-factor | 0.1979 |
Rwork | 0.195 |
R-free | 0.24280 |
Structure solution method | SAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.231 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELXDE |
Refinement software | REFMAC (5.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.180 | 2.840 |
High resolution limit [Å] | 2.700 | 2.700 |
Rpim | 0.054 | 0.559 |
Number of reflections | 14029 | 1374 |
<I/σ(I)> | 13.2 | 2 |
Completeness [%] | 99.3 | |
Redundancy | 6.6 | |
CC(1/2) | 0.968 | 0.817 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICROBATCH | 7 | 277 | 0.2 M NaSCN, 0.1 M HEPES pH 7.0, 22% PEG 3350 |