7QM2
Crystal structure of the PP1/PTG/beta-cyclodextrin ternary complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ELETTRA BEAMLINE 11.2C |
Synchrotron site | ELETTRA |
Beamline | 11.2C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-05-14 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.0000 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 153.600, 153.600, 285.620 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 120.585 | 2.883 |
High resolution limit [Å] | 2.685 | 2.685 |
Rmerge | 0.363 | |
Rpim | 0.090 | |
Number of reflections | 36706 | 1837 |
<I/σ(I)> | 13.3 | |
Completeness [%] | 66.3 | 18.9 |
Redundancy | 32 | 33.9 |
CC(1/2) | 0.997 | 0.422 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 277 | 0.1 M sodium acetate, 1 M sodium malonate |