7PS9
Cereblon isoform 4 from Magnetospirillum gryphiswaldense in complex with Iberdomide (CC-220)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-03-14 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9999 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 56.001, 58.850, 88.583 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.760 - 1.800 |
R-factor | 0.1956 |
Rwork | 0.193 |
R-free | 0.24620 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4v2y |
RMSD bond length | 0.008 |
RMSD bond angle | 1.546 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0266) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.760 | 1.910 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.135 | 1.542 |
Rmeas | 0.141 | 1.611 |
Number of reflections | 27318 | 4220 |
<I/σ(I)> | 11.24 | 1.21 |
Completeness [%] | 97.7 | 94.9 |
Redundancy | 12.5 | 11 |
CC(1/2) | 0.998 | 0.845 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.5 M (NH4)H2PO4 |