Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ELETTRA BEAMLINE 11.2C |
| Synchrotron site | ELETTRA |
| Beamline | 11.2C |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2021-06-06 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.971800 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 62.270, 71.340, 121.410 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 46.920 - 1.461 |
| Rwork | 0.177 |
| R-free | 0.20500 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1jv0 |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.825 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | REFMAC |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 46.920 | 1.500 |
| High resolution limit [Å] | 1.460 | 1.460 |
| Rmerge | 0.063 | 1.191 |
| Rmeas | 0.065 | 1.241 |
| Number of reflections | 94318 | 6929 |
| <I/σ(I)> | 20 | |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 12.46 | 12.63 |
| CC(1/2) | 0.999 | 0.838 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 28-31% PEG4000, 0.2 M Sodium acetate, 0.1 M Tris pH 8.5-9.0 |
