Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 93 |
Detector technology | PIXEL |
Collection date | 2015-11-05 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.999990 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 170.970, 202.310, 251.660 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.850 |
High resolution limit [Å] | 2.750 | 2.750 |
Number of reflections | 225685 | 16539 |
<I/σ(I)> | 11.99 | |
Completeness [%] | 100.0 | |
Redundancy | 13.8 | |
CC(1/2) | 0.990 | 0.680 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 277.15 | 0.1 M Ammonium tartrate dibasic pH 7.0, 12% (w/v) PEG 3350 |