Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 93 |
Detector technology | PIXEL |
Collection date | 2016-02-14 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 0.99 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 137.070, 110.440, 158.210 |
Unit cell angles | 90.00, 93.11, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.007 | 3.340 |
High resolution limit [Å] | 3.150 | 3.150 |
Rmeas | 0.320 | 1.050 |
Number of reflections | 81593 | 12843 |
<I/σ(I)> | 9.49 | 1.6 |
Completeness [%] | 99.6 | |
Redundancy | 7.03 | |
CC(1/2) | 0.980 | 0.530 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277.15 | 0.1 M Ammonium citrate tribasic pH 7.0, 12% (w/v) PEG 3350 |