Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 93 |
Detector technology | PIXEL |
Collection date | 2017-10-13 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 0.99 |
Spacegroup name | P 1 |
Unit cell lengths | 114.588, 114.614, 142.373 |
Unit cell angles | 92.31, 106.00, 111.41 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.200 | 2.810 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmeas | 0.170 | 0.740 |
Number of reflections | 181005 | 55527 |
<I/σ(I)> | 5.9 | 1.4 |
Completeness [%] | 94.8 | |
Redundancy | 1.8 | |
CC(1/2) | 0.980 | 0.610 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277.15 | 0.1 M sodium malonate (pH 5.5), 14.4% PEG 3350 |