7P9I
Structure of E.coli RlmJ in complex with an RNA conjugate (GAA-SAM)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-09-29 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.978 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 62.480, 57.590, 79.440 |
Unit cell angles | 90.00, 98.14, 90.00 |
Refinement procedure
Resolution | 42.148 - 1.594 |
R-factor | 0.1897 |
Rwork | 0.188 |
R-free | 0.22320 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6qdx |
Data reduction software | XDS |
Data scaling software | Aimless (0.7.4) |
Phasing software | MOLREP |
Refinement software | PHENIX (1.16_3549) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 46.460 | 46.460 | 1.640 |
High resolution limit [Å] | 1.590 | 7.130 | 1.590 |
Rmerge | 0.085 | 0.025 | 1.418 |
Rmeas | 0.092 | 0.027 | 1.541 |
Rpim | 0.035 | 0.011 | 0.593 |
Total number of observations | 507892 | 5497 | 32747 |
Number of reflections | 74189 | 884 | 5089 |
<I/σ(I)> | 14.5 | 43.8 | 1.3 |
Completeness [%] | 99.4 | 99.4 | 92.3 |
Redundancy | 6.8 | 6.2 | 6.4 |
CC(1/2) | 0.999 | 1.000 | 0.534 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.5 | 293 | 0.1 M BIS-TRIS pH 6.5, 20% w/v PEG MME 5000 |