7P72
The PDZ domain of SNX27 complexed with the PDZ-binding motif of MERS-E
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-03-17 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 61.170, 83.950, 106.590 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.000 | 2.210 |
High resolution limit [Å] | 2.150 | 2.150 |
Rmeas | 0.252 | 2.260 |
Number of reflections | 30598 | 2226 |
<I/σ(I)> | 8.97 | 1.34 |
Completeness [%] | 99.9 | 100 |
Redundancy | 13.2 | 13.5 |
CC(1/2) | 0.998 | 0.719 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 10% polyethylene glycol 8000, 100 mM imidazole buffered at pH 8.0 |