7OX5
hIL-9:hIL-9Ra complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-11-19 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.98 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 85.450, 107.810, 159.550 |
Unit cell angles | 90.00, 90.77, 90.00 |
Refinement procedure
Resolution | 47.690 - 3.090 |
R-factor | 0.2228 |
Rwork | 0.220 |
R-free | 0.27960 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2b5i |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.690 | 3.270 |
High resolution limit [Å] | 3.090 | 3.090 |
Number of reflections | 52814 | 8141 |
<I/σ(I)> | 11.39 | |
Completeness [%] | 98.9 | |
Redundancy | 3.5 | |
CC(1/2) | 0.998 | 0.281 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 293 | 0.1 M ammonium sulfate, 0.1 M TRIS, pH 5.6, 18% PEG 1500 |