7OUZ
Human OMPD-domain of UMPS in complex with 6-hydroxy-UMP at 0.9 Angstroms resolution, crystal 1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P14 (MX2) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P14 (MX2) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-04-04 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.7653 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 77.896, 116.425, 61.968 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.300 - 0.900 |
R-factor | 0.11 |
Rwork | 0.110 |
R-free | 0.11960 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2qcc |
Data reduction software | XDS |
Data scaling software | XSCALE |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 30.300 | 30.300 | 0.920 |
High resolution limit [Å] | 0.900 | 4.020 | 0.900 |
Rmerge | 0.036 | 0.024 | 0.856 |
Rmeas | 0.042 | 0.029 | 1.056 |
Total number of observations | 701093 | ||
Number of reflections | 200348 | 2026 | 13775 |
<I/σ(I)> | 15.25 | 41.48 | 1.23 |
Completeness [%] | 96.8 | 80.5 | 90.6 |
Redundancy | 3.499 | 3.303 | 2.658 |
CC(1/2) | 0.999 | 0.996 | 0.530 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.8 | 293 | Tris/HCl, ammonium sulfate, glutathione |