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7O9J

Crystal structure of DyP-type peroxidase from Dictyostelium discoideum in complex with an activated form of oxygen

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID29
Synchrotron siteESRF
BeamlineID29
Temperature [K]100
Detector technologyPIXEL
Collection date2012-12-01
DetectorDECTRIS PILATUS 6M
Wavelength(s)0.91985
Spacegroup nameP 41 21 2
Unit cell lengths141.030, 141.030, 95.560
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution45.250 - 1.700
R-factor0.1471
Rwork0.146
R-free0.16530
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2iiz
RMSD bond length0.006
RMSD bond angle1.098
Data reduction softwareXDS
Data scaling softwareSADABS
Phasing softwarePHASER
Refinement softwarePHENIX (1.17.1_3660)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]47.7801.790
High resolution limit [Å]1.7001.700
Rmerge0.0310.360
Number of reflections10581014967
<I/σ(I)>18.462.85
Completeness [%]100.0100
Redundancy26.625.44
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION72932.4 M sodium malonate pH 7.0

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