7NPM

X-ray structure of the adduct formed upon reaction of oxaliplatin with human angiogenin

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ELETTRA BEAMLINE 11.2C
Synchrotron site	ELETTRA
Beamline	11.2C
Temperature [K]	100
Detector technology	PIXEL
Collection date	2020-11-19
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.96
Spacegroup name	P 21 21 2
Unit cell lengths	37.720, 85.890, 33.390
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	42.940 - 1.860
Rwork	0.178
R-free	0.25370
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	5eop
RMSD bond length	0.010
RMSD bond angle	1.628
Data reduction software	MOSFLM
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	REFMAC (5.8.0258)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	42.945	1.890
High resolution limit [Å]	1.860	1.860
Rmerge	0.171	1.220
Rpim	0.052	0.387
Number of reflections	9691	475
<I/σ(I)>	10.5	2.5
Completeness [%]	99.9	100
Redundancy	11.8	10.7
CC(1/2)	0.995	0.803

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	5.1	298	10 % PEG6K, 20 mM sodium citrate pH 5.1, 0.2 M sodium/potassium tartrate