7NBI
Crystal structure of a monomeric FLT3 Ligand variant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-03-25 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97625 |
Spacegroup name | P 1 |
Unit cell lengths | 28.300, 43.490, 46.360 |
Unit cell angles | 82.82, 85.41, 85.10 |
Refinement procedure
Resolution | 18.420 - 1.650 |
R-factor | 0.1662 |
Rwork | 0.164 |
R-free | 0.20260 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ete |
RMSD bond length | 0.018 |
RMSD bond angle | 1.490 |
Data reduction software | XDS (VERSION Jan 31, 2020) |
Data scaling software | XDS (VERSION Jan 31, 2020) |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.1_4122) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 18.640 | 1.709 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmeas | 0.077 | 0.567 |
Number of reflections | 70278 | 4053 |
<I/σ(I)> | 10.6 | 2.33 |
Completeness [%] | 94.9 | 89.2 |
Redundancy | 8.81 | 2.37 |
CC(1/2) | 0.996 | 0.728 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 293 | 2.0 M ammonium sulfate, 0.1 M HEPES |