7MQY
Zebrafish CNTN4 APLP2 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2019-10-19 |
Detector | RAYONIX MX300-HS |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 61.660, 44.980, 99.829 |
Unit cell angles | 90.00, 95.84, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 99.310 | 2.560 |
High resolution limit [Å] | 2.460 | 2.460 |
Rmerge | 0.090 | 0.597 |
Rmeas | 0.096 | 0.646 |
Rpim | 0.035 | 0.243 |
Number of reflections | 20199 | 2266 |
<I/σ(I)> | 15.6 | 3.9 |
Completeness [%] | 100.0 | 99.9 |
Redundancy | 7.4 | 7 |
CC(1/2) | 0.998 | 0.909 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 100 mM Na-acetate pH 5.2, 30% (w/v) PEG 8,000 |