7MOV
PTP1B 1-301 F225Y-R199N mutations
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-01-25 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97946 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 114.359, 90.102, 74.490 |
Unit cell angles | 90.00, 110.93, 90.00 |
Refinement procedure
Resolution | 37.820 - 1.650 |
R-factor | 0.1667 |
Rwork | 0.165 |
R-free | 0.19330 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5k9v |
RMSD bond length | 0.018 |
RMSD bond angle | 1.464 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX (1.19.1_4122) |
Refinement software | PHENIX (1.19.1_4122) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.820 | 1.680 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.063 | 1.004 |
Number of reflections | 80907 | 3446 |
<I/σ(I)> | 16.8 | 1.7 |
Completeness [%] | 95.4 | |
Redundancy | 7.2 | |
CC(1/2) | 0.999 | 0.732 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 0.1 M Tris pH 7.4, 0.2 M Magnesium Chloride, 21.5% PEG 8000 |