7MOU
PTP1B F225Y-R199N-L195R
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-04-08 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97946 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 88.427, 88.427, 72.459 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 38.290 - 1.480 |
R-factor | 0.1719 |
Rwork | 0.172 |
R-free | 0.18010 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5k9v |
RMSD bond length | 0.014 |
RMSD bond angle | 1.318 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX (1.18.2_3874) |
Refinement software | PHENIX (1.19.1_4122) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.290 | 1.500 |
High resolution limit [Å] | 1.480 | 1.480 |
Rmerge | 0.073 | 1.047 |
Number of reflections | 54819 | 2649 |
<I/σ(I)> | 19.2 | 2.2 |
Completeness [%] | 99.8 | |
Redundancy | 11.1 | |
CC(1/2) | 0.997 | 0.772 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 0.2 M MgCl2, .1 M Tris pH 7.8, 16.5% PEG |