7MC5
Crystal structure of the SARS-CoV-2 ExoN-nsp10 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-12-15 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9791 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 63.735, 67.480, 111.249 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 57.700 - 1.640 |
R-factor | 0.1678 |
Rwork | 0.166 |
R-free | 0.19690 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5c8t |
RMSD bond length | 0.011 |
RMSD bond angle | 1.098 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.32) |
Phasing software | PHASER |
Refinement software | PHENIX (1.19_4085) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 111.250 | 111.250 | 1.670 |
High resolution limit [Å] | 1.640 | 8.990 | 1.640 |
Rmerge | 0.114 | 0.036 | 1.203 |
Rmeas | 0.129 | 0.041 | 1.377 |
Rpim | 0.060 | 0.020 | 0.658 |
Total number of observations | 1664 | 9396 | |
Number of reflections | 58701 | 432 | 2330 |
<I/σ(I)> | 12.2 | 40.5 | 1.3 |
Completeness [%] | 98.9 | 98.8 | 81.3 |
Redundancy | 4.3 | 3.9 | 4 |
CC(1/2) | 0.996 | 0.998 | 0.536 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 295 | di-ammonium tartrate, pH 7.0, PEG 3350 |