7M4T
Menin bound to M-1121
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-D |
Synchrotron site | APS |
Beamline | 21-ID-D |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-04-17 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 1.12714 |
Spacegroup name | I 41 |
Unit cell lengths | 153.520, 153.520, 81.930 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.550 - 2.740 |
R-factor | 0.203 |
Rwork | 0.202 |
R-free | 0.21500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6wnh |
RMSD bond length | 0.008 |
RMSD bond angle | 0.960 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.790 |
High resolution limit [Å] | 2.740 | 7.430 | 2.740 |
Rmerge | 0.081 | 0.034 | 0.704 |
Rmeas | 0.090 | 0.037 | 0.784 |
Rpim | 0.039 | 0.016 | 0.341 |
Total number of observations | 134851 | ||
Number of reflections | 24922 | 1308 | 1105 |
<I/σ(I)> | 10.4 | ||
Completeness [%] | 98.8 | 99.4 | 89.8 |
Redundancy | 5.4 | 5.5 | 4.7 |
CC(1/2) | 0.995 | 0.806 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 2.0 M NaCl, 90.9 M Bis-Tris pH 6.5, 0.182 M MgCl2, 10 mM Pr Acetate |