7LWB
Crystal Structure of phospho-Rab8a with the RH2 domain (117-165) of RILPL2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-07-28 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 0.97918 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 62.773, 68.430, 128.100 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.260 - 1.900 |
R-factor | 0.2209 |
Rwork | 0.219 |
R-free | 0.26680 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6rir |
RMSD bond length | 0.014 |
RMSD bond angle | 1.329 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.260 | 1.968 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.057 | 4.301 |
Rmeas | 4.610 | |
Rpim | 0.021 | 1.620 |
Number of reflections | 21414 | 1964 |
<I/σ(I)> | 16.79 | 0.35 |
Completeness [%] | 96.0 | 90.3 |
Redundancy | 8.6 | 7.9 |
CC(1/2) | 0.999 | 0.540 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 288 | 150mM DL-Malic acid, 20% PEG3350 |