7LQN
Glucosamine-6-phosphate Deaminase from H. influenzae
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-07-01 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9786 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 103.405, 144.300, 131.143 |
Unit cell angles | 90.00, 92.07, 90.00 |
Refinement procedure
Resolution | 47.490 - 3.000 |
R-factor | 0.1959 |
Rwork | 0.194 |
R-free | 0.24200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1dea |
Data reduction software | XDS (VERSION Jan 26, 2018) |
Data scaling software | Aimless (0.6.3) |
Phasing software | PHENIX (1.19) |
Refinement software | PHENIX (1.19) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.670 | 3.060 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.170 | 0.530 |
Rmeas | 0.203 | 0.629 |
Rpim | 0.109 | 0.336 |
Total number of observations | 256858 | |
Number of reflections | 76608 | 4516 |
<I/σ(I)> | 6.4 | |
Completeness [%] | 99.5 | 99.4 |
Redundancy | 3.4 | 3.4 |
CC(1/2) | 0.972 | 0.845 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 291 | 2 % w/v Tasciminate pH 5.0, 0.1 M Sodium Citrate tribasic pH 5.6, 16 % PEG 3350 with 0.1 M Strontium Chloride. 6H2O as additive |