7LML
Receptor for Advanced Glycation End Products VC1 domain in complex with 3-(3-(((3-(4-Carboxyphenoxy)benzyl)oxy)methyl)phenyl)-1H-indole-2-carboxylic acid
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 12.3.1 |
Synchrotron site | ALS |
Beamline | 12.3.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-05-12 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9795 |
Spacegroup name | P 62 |
Unit cell lengths | 102.478, 102.478, 102.158 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 40.700 - 2.150 |
R-factor | 0.2131 |
Rwork | 0.212 |
R-free | 0.23510 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4lp4 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.768 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.1_4122) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.700 | 2.532 |
High resolution limit [Å] | 2.150 | 2.150 |
Rmeas | 0.072 | 0.124 |
Rpim | 0.026 | 0.044 |
Number of reflections | 32950 | 12707 |
<I/σ(I)> | 16.2 | 3.66 |
Completeness [%] | 99.3 | 99.1 |
Redundancy | 4 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 277 | 2.5 M NaOAc (pH 7.5) |