7KXW
Crystal structure of DCLK1-KD in complex with DCLK1-IN-1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-03-21 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9537 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 143.950, 61.714, 65.312 |
Unit cell angles | 90.00, 103.04, 90.00 |
Refinement procedure
Resolution | 44.288 - 3.002 |
R-factor | 0.2031 |
Rwork | 0.200 |
R-free | 0.25970 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5jzj |
Data scaling software | Aimless (0.5.32) |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 44.290 | 44.290 | 3.180 |
High resolution limit [Å] | 3.000 | 9.010 | 3.000 |
Rmerge | 0.156 | 0.057 | 0.775 |
Rmeas | 0.169 | 0.062 | 0.839 |
Rpim | 0.064 | 0.023 | 0.316 |
Total number of observations | 76277 | 2942 | 11337 |
Number of reflections | 11200 | 439 | 1669 |
<I/σ(I)> | 11.4 | 25.6 | 3.6 |
Completeness [%] | 98.8 | 99.2 | 93 |
Redundancy | 6.8 | 6.7 | 6.8 |
CC(1/2) | 0.996 | 0.997 | 0.819 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 7.25 | 298 | PEG400, ammonium sulfphate, Hepes |