7KX8
Crystal structure of DCLK1-Cter in complex with FMF-03-055-1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-08-19 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9537 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 65.920, 62.430, 72.080 |
Unit cell angles | 90.00, 96.07, 90.00 |
Refinement procedure
Resolution | 71.676 - 3.100 |
R-factor | 0.1957 |
Rwork | 0.193 |
R-free | 0.25090 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5jzj |
RMSD bond length | 0.003 |
RMSD bond angle | 0.658 |
Data scaling software | Aimless (0.5.8) |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 71.680 | 71.680 | 3.310 |
High resolution limit [Å] | 3.100 | 8.770 | 3.100 |
Rmerge | 0.236 | 0.055 | 0.927 |
Rmeas | 0.263 | 0.061 | 1.032 |
Rpim | 0.115 | 0.026 | 0.444 |
Total number of observations | 50639 | 2388 | 9282 |
Number of reflections | 10702 | 512 | 1926 |
<I/σ(I)> | 7.3 | 16.9 | 2.6 |
Completeness [%] | 99.5 | 99.7 | 99.8 |
Redundancy | 4.7 | 4.7 | 4.8 |
CC(1/2) | 0.980 | 0.998 | 0.709 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 7.25 | 298 | PEG400, ammonium sulfphate, Hepes |