7KNX
Crystal structure of SND1 in complex with C-26-A6
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | LIQUID ANODE |
| Source details | BRUKER METALJET |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-12-07 |
| Detector | Bruker PHOTON II |
| Wavelength(s) | 1.34 |
| Spacegroup name | P 1 |
| Unit cell lengths | 61.127, 81.880, 81.882 |
| Unit cell angles | 83.77, 70.89, 70.91 |
Refinement procedure
| Resolution | 30.000 - 2.700 |
| R-factor | 0.2632 |
| Rwork | 0.260 |
| R-free | 0.32900 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.527 |
| Data scaling software | SCALEPACK |
| Refinement software | REFMAC (5.8.0189) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 2.770 |
| High resolution limit [Å] | 2.700 | 2.700 |
| Rmerge | 1.000 | 1.000 |
| Number of reflections | 37571 | 2776 |
| <I/σ(I)> | 5.5 | |
| Completeness [%] | 96.5 | 95.8 |
| Redundancy | 5.5 | 1.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.2 | 293 | 0.1 MES-NaOH pH 6.2, 0.9 M trisodium citrate |
