7KKH
P1A4 Fab in complex with ARS1620
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-09-27 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.1158 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 103.782, 71.302, 86.793 |
Unit cell angles | 90.00, 90.66, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 58.770 | 2.072 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 42846 | 4212 |
<I/σ(I)> | 7.75 | |
Completeness [%] | 99.4 | |
Redundancy | 10.2 | |
CC(1/2) | 0.996 | 0.490 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293.15 | 0.1 M HEPES pH 7.5, 70 % MPD |