7KF4
Crystal structure from SARS-CoV-2 NendoU NSP15
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX IV BEAMLINE BioMAX |
Synchrotron site | MAX IV |
Beamline | BioMAX |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-06-13 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.976254 |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 85.125, 151.163, 199.242 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.160 - 2.610 |
R-factor | 0.22 |
Rwork | 0.219 |
R-free | 0.24600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6x1b |
RMSD bond length | 0.010 |
RMSD bond angle | 1.110 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.160 | 2.703 |
High resolution limit [Å] | 2.610 | 2.610 |
Number of reflections | 78886 | 7756 |
<I/σ(I)> | 8.24 | |
Completeness [%] | 99.7 | |
Redundancy | 13.8 | |
CC(1/2) | 0.998 | 0.527 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 5 | 293 | 0.1 M trisodium citrate pH 5, 14 % w/v PEG6000 |