7K3S

Solution NMR Structure of the Coiled-coil BRCA1-PALB2 Heterodimer

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE		800

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC NH2 only
11	1	1	3D 1H-13C NOESY
12	1	1	3D 1H-15N NOESY
13	1	2	2D 1H-15N HSQC NH2 only
14	1	2	3D HNCA
15	1	2	2D 1H-13C HSQC aliphatic
16	1	2	3D HN(CO)CA
17	1	2	3D HCCH-TOCSY
18	1	2	3D HNCACB
19	1	2	3D CBCA(CO)NH
2	1	1	2D 1H-13C HSQC aliphatic
20	1	2	3D HNCO
21	1	2	3D HBHA(CO)NH
22	1	2	3D 1H-15N NOESY
23	1	2	3D 1H-13C NOESY
25	1	1	3D HBHA(CO)NH
3	1	1	3D HNCA
4	1	1	3D HN(CO)CA
5	1	1	3D HCCH-TOCSY
6	1	1	3D HNCACB
7	1	1	3D CBCA(CO)NH
8	1	1	3D HNCO
9	1	1	3D 1H-15N TOCSY

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	6.5	1	293

Conformers

Conformers Calculated Total Number	200
Conformers Submitted Total Number	15