7JL4
Crystal structure of TRIM65 PSpry domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS-II BEAMLINE 17-ID-1 |
Synchrotron site | NSLS-II |
Beamline | 17-ID-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-10-14 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.9201 |
Spacegroup name | P 32 |
Unit cell lengths | 76.269, 76.269, 82.720 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 38.130 - 1.920 |
R-factor | 0.1695 |
Rwork | 0.168 |
R-free | 0.20870 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6fln |
RMSD bond length | 0.009 |
RMSD bond angle | 1.612 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2-3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.130 | 1.990 |
High resolution limit [Å] | 1.920 | 1.920 |
Number of reflections | 41070 | 4050 |
<I/σ(I)> | 13.34 | |
Completeness [%] | 99.9 | |
Redundancy | 5.3 | |
CC(1/2) | 0.996 | 0.952 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG3350, Bicine, pH 9.0 |