Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

7G1V

Crystal Structure of human FABP4 in complex with 3-[(2-sulfanylphenyl)carbamoyl]bicyclo[2.2.1]heptane-2-carboxylic acid

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X10SA
Synchrotron siteSLS
BeamlineX10SA
Temperature [K]100
Detector technologyPIXEL
Collection date2012-02-05
DetectorPSI PILATUS 6M
Wavelength(s)0.700030
Spacegroup nameP 21 21 21
Unit cell lengths32.366, 53.770, 75.641
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution37.820 - 1.020
R-factor0.1348
Rwork0.134
R-free0.16030
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)inhouse model
RMSD bond length0.022
RMSD bond angle2.193
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwarePHASER
Refinement softwareREFMAC (5.7.0018)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]37.82037.8201.050
High resolution limit [Å]1.0204.5601.020
Rmerge0.0570.0301.039
Rmeas0.0640.0331.125
Total number of observations442940
Number of reflections671418764848
<I/σ(I)>14.5650.141.95
Completeness [%]98.698.897.2
Redundancy6.526.016.688
CC(1/2)0.9990.9990.722
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP7293protein in 25mM Tris/HCl pH 7.5 100mM NaCl, see also PMID 27658368

223532

PDB entries from 2024-08-07

PDB statisticsPDBj update infoContact PDBjnumon