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7EOD

MITF HLHLZ Delta AKE

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRF BEAMLINE BL19U1
Synchrotron siteSSRF
BeamlineBL19U1
Temperature [K]100
Detector technologyPIXEL
Collection date2020-07-07
DetectorDECTRIS PILATUS3 6M
Wavelength(s)0.97852
Spacegroup nameP 1
Unit cell lengths33.020, 52.880, 55.470
Unit cell angles82.64, 85.49, 71.85
Refinement procedure
Resolution39.160 - 1.900
R-factor0.1907
Rwork0.188
R-free0.23790
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)7d8r
Data reduction softwareDIALS
Data scaling softwareAimless (0.7.4)
Phasing softwareMOLREP
Refinement softwarePHENIX (1.13_2998)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]40.00040.0001.940
High resolution limit [Å]1.9009.1101.900
Rmerge0.0740.0210.684
Rmeas0.0870.0240.804
Rpim0.0450.0120.419
Number of reflections498122351705
<I/σ(I)>11.7
Completeness [%]93.992.993.7
Redundancy3.63.63.5
CC(1/2)0.9980.9990.817
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP2911.8 M Ammonium citrate pH 7.0

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