7EJW
Crystal structure of FleN in complex with FleQ AAA+ doamain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID30B |
Synchrotron site | ESRF |
Beamline | ID30B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-06-26 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97951 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 64.218, 153.926, 64.568 |
Unit cell angles | 90.00, 95.03, 90.00 |
Refinement procedure
Resolution | 64.319 - 1.980 |
R-factor | 0.1808 |
Rwork | 0.179 |
R-free | 0.21800 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.034 |
Data reduction software | DIALS |
Data scaling software | SCALA |
Phasing software | AutoSol |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 77.000 | 2.020 |
High resolution limit [Å] | 1.980 | 1.980 |
Rmerge | 0.092 | 0.564 |
Rmeas | 0.686 | |
Rpim | 0.062 | 0.386 |
Number of reflections | 86189 | 4574 |
<I/σ(I)> | 7.6 | 1.9 |
Completeness [%] | 99.5 | 99.5 |
Redundancy | 3.1 | |
CC(1/2) | 0.984 | 0.556 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 277 | 10% PEG 8000, 0.1M imidazole, 0.2M calcium acetate |