7EHW
BRD4-BD1 in complex with LT-642-602
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-12-10 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9793 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 32.160, 47.300, 82.340 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 31.054 - 1.650 |
R-factor | 0.21 |
Rwork | 0.208 |
R-free | 0.24650 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4qr4 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3235) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.010 | 1.680 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.452 | |
Number of reflections | 14169 | 679 |
<I/σ(I)> | 4.8 | |
Completeness [%] | 91.0 | |
Redundancy | 4 | |
CC(1/2) | 0.980 | 0.371 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 295 | 4 M sodium formate |