7E4W
Human Transcriptional Co-activator PC4 (C-terminal Domain) in space group P1211
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | RRCAT INDUS-2 BEAMLINE PX-BL21 |
Synchrotron site | RRCAT INDUS-2 |
Beamline | PX-BL21 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2019-04-02 |
Detector | RAYONIX MX-225 |
Wavelength(s) | 0.97947 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 49.012, 166.844, 108.309 |
Unit cell angles | 90.00, 93.27, 90.00 |
Refinement procedure
Resolution | 108.130 - 2.900 |
R-factor | 0.2301 |
Rwork | 0.228 |
R-free | 0.27760 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1pcf |
RMSD bond length | 0.011 |
RMSD bond angle | 1.534 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 108.130 | 3.000 |
High resolution limit [Å] | 2.900 | 2.900 |
Number of reflections | 38333 | 3798 |
<I/σ(I)> | 7.7 | 1.41 |
Completeness [%] | 99.5 | 99.84 |
Redundancy | 3.8 | |
CC(1/2) | 0.988 | 0.614 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 285 | 20% MPD, 150-200 MM NACL, Phosphate Buffer (PH 5-5.2) |