7D26
Hsp90 alpha N-terminal domain in complex with a 8 compund
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-03-29 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0000 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 67.613, 89.389, 98.216 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.742 - 1.750 |
R-factor | 0.1955 |
Rwork | 0.193 |
R-free | 0.22790 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5h22 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.16_3549) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.810 |
High resolution limit [Å] | 1.748 | 3.770 | 1.750 |
Rmerge | 0.093 | 0.070 | 0.277 |
Number of reflections | 29933 | 3177 | 2886 |
<I/σ(I)> | 12 | ||
Completeness [%] | 98.6 | 99.5 | 96.2 |
Redundancy | 5.5 | 7.5 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 295 | 1.0M ammonium Sulfate, 0.1M Tris-HCl (pH8.5) |