7D24
Hsp90 alpha N-terminal domain in complex with a 4B compund
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-02-20 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.00000 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 67.351, 89.891, 98.591 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.957 - 1.550 |
R-factor | 0.1811 |
Rwork | 0.180 |
R-free | 0.19800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5h22 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.16_3549) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.610 |
High resolution limit [Å] | 1.547 | 3.340 | 1.550 |
Rmerge | 0.040 | 0.031 | 0.206 |
Number of reflections | 42003 | 4506 | 3591 |
<I/σ(I)> | 20.7 | ||
Completeness [%] | 95.7 | 97.9 | 82.8 |
Redundancy | 6.4 | 7.7 | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 295 | 1.0M ammonium Sulfate, 0.1M Tris-HCl (pH8.5) |