7CPN
CRYSTAL STRUCTURE OF DODECAPRENYL DIPHOSPHATE SYNTHASE FROM THERMOBIFIDA FUSCA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-03-11 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 71.095, 137.878, 168.652 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.534 - 2.280 |
Rwork | 0.203 |
R-free | 0.23940 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1f75 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.410 |
Data reduction software | HKL-2000 |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.534 | 2.320 |
High resolution limit [Å] | 2.280 | 2.280 |
Rmerge | 0.059 | 0.385 |
Number of reflections | 77502 | 3826 |
<I/σ(I)> | 63.647 | 8.564 |
Completeness [%] | 100.0 | 100 |
Redundancy | 8.4 | 7.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 293 | 0.1 M citric acid sodium citrate pH 5.0, 0.7 M ammonium sulfate |