7C4V
MicroED structure of anorthic Vancomycin at 1.05 A resolution
Experimental procedure
| Collection date | 2019-06-01 |
| Spacegroup name | P 1 |
| Unit cell lengths | 13.970, 18.550, 23.860 |
| Unit cell angles | 109.52, 97.33, 106.58 |
Refinement procedure
| Resolution | 7.875 - 1.050 |
| R-factor | 0.2335 |
| Rwork | 0.232 |
| R-free | 0.26840 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1fvm |
| Refinement software | PHENIX (1.15_3459) |
Data quality characteristics
| Outer shell | |
| Low resolution limit [Å] | 1.100 |
| High resolution limit [Å] | 1.050 |
| Rmerge | 0.419 |
| Number of reflections | 852 |
| <I/σ(I)> | 3.04 |
| Completeness [%] | 66.9 |
| Redundancy | 6.83 |
| CC(1/2) | 0.949 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
